Effect of Low Solid/Liquid Ratio on Hydrothermal Synthesis of Hydroxyapatite with Green Template from Banana Flower (Musa acuminata Cavendish)

Authors

  • Ferli Septi Irwansyah Department of Chemistry Education, UIN Sunan Gunung Djati, Indonesia http://orcid.org/0000-0002-9613-2029
  • Alfi Ikhlasul Amal Department of Chemistry, Faculty of Science and Technology, UIN Sunan Gunung Djati, Indonesia
  • Eko Prabowo Hadisantoso Department of Chemistry, Faculty of Science and Technology, UIN Sunan Gunung Djati, Indonesia
  • Atiek Rostika Noviyanti Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Padjadjaran, Indonesia
  • Diana Rakhmawaty Eddy Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Padjadjaran, Indonesia
  • Azman Bin Ma'Amor Department of Chemistry, Universiti Malaya, Malaysia
  • Risdiana Risdiana Department of Physics, Faculty of Mathematics and Natural Sciences, Universitas Padjadjaran, Indonesia

DOI:

https://doi.org/10.15575/ak.v10i1.25262

Keywords:

Hydroxyapatite, hydrothermal, solid/liquid ratio, green template, banana flower

Abstract

Hydroxyapatite (HA) was successfully synthesized using the hydrothermal method. This study aimed to analyze the effect of a low solid/liquid ratio on the properties of HA crystals. HA synthesis was performed using chicken eggshells and the hydrothermal method at a temperature of 150°C. The solvent amount was kept constant, while the solid amount varied (half-reaction). The characteristics of HA were determined using XRD, FTIR, PSA, and SEM. The results showed that the purity and size of HA were influenced by a low solid/liquid ratio, while the crystallinity remained relatively unchanged, directly impacting the lattice parameter value. FTIR analysis revealed the absence of the O-H group in the sample with the low solid/liquid ratio. PSA results showed a smaller particle size of 0.995 µm for the sample with the low solid/liquid ratio. SEM results demonstrated a smaller particle size in the sample with a low solid/liquid ratio when observed at the same magnification

Author Biography

Ferli Septi Irwansyah, Department of Chemistry Education, UIN Sunan Gunung Djati

Scopus ID:57213520381

ORCID ID : 0000-0002-9613-2029

ResearcherID: B-8869-2017

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Published

2023-06-30

Issue

Vol. 10 No. 1 (2023): al Kimiya: Jurnal Ilmu Kimia dan Terapan

Section

Articles

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